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Topic: Phenylbutazone synthesis  (Read 12738 times)

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Offline orthoformate

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Re: Phenylbutazone synthesis
« Reply #15 on: July 07, 2016, 10:18:20 PM »
Quote from: anuradha on July 07, 2016, 07:28:45 PM
I have tried this method already but did not see any products thats why I was trying with acid. I wanted to make this compound quickly. I will try this procedure again. Thank you for your advice.

There is excellent precedent for this sodium method. I can help you through this procedure if you need.

Attached is a more in depth description of the Na/EtOH procedure (Open Source from ACS Supplemental Info) for a similar molecule.
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Offline anuradha

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Re: Phenylbutazone synthesis
« Reply #16 on: July 08, 2016, 11:15:43 PM »
Quote from: orthoformate on July 07, 2016, 10:18:20 PM
Quote from: anuradha on July 07, 2016, 07:28:45 PM
I have tried this method already but did not see any products thats why I was trying with acid. I wanted to make this compound quickly. I will try this procedure again. Thank you for your advice.

There is excellent precedent for this sodium method. I can help you through this procedure if you need.

Attached is a more in depth description of the Na/EtOH procedure (Open Source from ACS Supplemental Info) for a similar molecule.
I will proceed this procedure, thanks a lot. I will let you the result.
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