March 28, 2024, 02:18:34 PM
Forum Rules: Read This Before Posting


Topic: triethyl amine purfication after column  (Read 1224 times)

0 Members and 1 Guest are viewing this topic.

Offline saubanzaheer

  • Very New Member
  • *
  • Posts: 1
  • Mole Snacks: +0/-0
triethyl amine purfication after column
« on: April 15, 2014, 11:41:25 AM »
I purified my compound possess one free NH2 group on column by using triethyl amine. Now I have problem because the TEA strong signal in proton NMR is appeared along with my compound. Can any one help me how to remove this from my compound.

Offline Archer

  • Chemist
  • Sr. Member
  • *
  • Posts: 1001
  • Mole Snacks: +85/-20
  • Gender: Male
Re: triethyl amine purfication after column
« Reply #1 on: April 15, 2014, 03:22:57 PM »
What is your molecule with one amine? You could use high vacuum if it's not too volatile.
“ I love him. He's hops. He's barley. He's protein. He's a meal. ”

Denis Leary.

Sponsored Links