March 28, 2024, 05:53:01 PM
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Topic: Synthesis of an aflatoxin-like compound  (Read 7403 times)

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Offline phth

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Re: Synthesis of an aflatoxin-like compound
« Reply #15 on: August 19, 2015, 11:54:26 AM »
I would try to use SePh instead of SPh.  Should work cold using H2O2 in a dipolar solvent(-->SeO2Ph), and then base such as K3PO4, or DABCO/.  glyme for example can be used as a solvent

Offline Rutherford

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Re: Synthesis of an aflatoxin-like compound
« Reply #16 on: August 19, 2015, 02:49:16 PM »
Great idea. Now the only piece left is to synthesize the protected diol with SePh instead of SPh.

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