Is mercury (I) soluble under those conditions? Mercury (II) is soluble in water. Mercury (I) is only slightly soluble, and prone to oxidation.
What is the analytical test? ICP, or flame AA, or gravimetric reaction, or what?
PeaGreen36: offered an idea. Do you think its a good one? Why or why not?
testing method is 6M HCl
That is not a testing method.