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Topic: index reflections h, k, l base factor  (Read 1997 times)

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Offline CHEKAL

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index reflections h, k, l base factor
« on: December 12, 2012, 01:26:26 PM »
how would i index reflections from xray diffraction using the base factor? i have an impossible reflection at 1.5 with the given data, the base factor has be calculated with a given reflection.

Offline Gibbs

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Re: index reflections h, k, l base factor
« Reply #1 on: December 14, 2012, 04:56:53 PM »
You need a new base factor. So, your smallest 2θ is giving a ratio of 1, you now need to change that to a ratio of 2. The Miller indices will change from 100 to 110. Now you can calculate a new base factor by taking sin2θ/2 This is new base factor. Then divide your sin2θ for the 1.5 ratio and you should then get an integer or close to integer value.

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