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Chemistry Forums for Students => Analytical Chemistry Forum => Topic started by: JCopping on June 22, 2016, 09:08:40 AM

Title: Bi in waters via ICP OES
Post by: JCopping on June 22, 2016, 09:08:40 AM
Hi
 Totally new to this forum, so please bear with me.
 I'm currently involved in a water analysis project and am having some issues measuring Bi with our ICP OES. The background is very 'noisy' making it difficult to attain a good clear peak.
 I'm using wavelength 223.0nm. My analysis is using a Pb and Bi combined standard set with a matrix of distilled water and 1% nitric acid.
 My question is, as my sample concentrations are <20ppb, is it likely that standard addition is my only option to get the best results?

 Any suggestions would be great.
 Thanks
 Jo