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Topic: finding relible method for hydroxylation  (Read 2646 times)

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Offline ajam

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finding relible method for hydroxylation
« on: September 19, 2006, 08:46:19 AM »
hi,
i want to do hydroxylation of 3-bromo-4,5-methylenedioxybenzaldehyde.
can anybody suggest me reliable method. i tried two methods. i will give references of these methods
1)Jacob Peyton and et al, Synth.Commun. 11,12,1981,969-978.
2)Achintya k. Sinhababu and et al, JOC, Vol.48,No.12, 1983,1941-1944.
by using first reference i got low yield around 25% and second reference didn't give required product.
so anybody can give me any right method with good yield to get desired product.

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