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Chemistry Forums for Students => Undergraduate General Chemistry Forum => Topic started by: Pjedi on December 15, 2012, 06:34:22 AM

Title: weighing stable isotopes using acurate balance
Post by: Pjedi on December 15, 2012, 06:34:22 AM
Hi, For a certain experiment I need to weigh enriched stable isotopes very accurately. Because of the high cost of this isotopes I can't take any bigger amount to weigh them accurately.

In my case, I need 4,173 mg of Ni 62 which is enriched for 98,2 %. I have trained to get the weight accurately using normal Ni and a satorius E2, which s able to measure weight accurately until 1 µg . So far the weight has an error for at least  10%.

Did anyone have the same problem? I would appreciate all kind of hints.



Title: Re: weighing stable isotopes using acurate balance
Post by: curiouscat on December 15, 2012, 07:09:26 AM
In my case, I need 4,173 mg of Ni 62 which is enriched for 98,2 %. I have trained to get the weight accurately using normal Ni and a satorius E2, which s able to measure weight accurately until 1 µg . So far the weight has an error for at least  10%.

How did you measure / quantify this error?

Quote
For a certain experiment I need to weigh enriched stable isotopes very accurately.

How accurately do you need to measure.
Title: Re: weighing stable isotopes using acurate balance
Post by: Pjedi on December 18, 2012, 04:47:01 AM




In my case, I need 4,173 mg of Ni 62 which is enriched for 98,2 %. I have trained to get the weight accurately using normal Ni and a satorius E2, which s able to measure weight accurately until 1 µg . So far the weight has an error for at least  10%.

How did you measure / quantify this error?

I just picked some natural abundant Ni and some weighing scales and started repeating the same experiment 5 times.

Quote
For a certain experiment I need to weigh enriched stable isotopes very accurately.

How accurately do you need to measure.

I want error below 2%
Title: Re: weighing stable isotopes using acurate balance
Post by: JGK on December 18, 2012, 03:02:42 PM
For that level of accuracy you will need a 6 decimal place balance (Sartorius ME36 or equivalent)