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Chemistry Forums for Students => Organic Chemistry Forum => Organic Chemistry Forum for Graduate Students and Professionals => Topic started by: black_kitty on May 13, 2008, 12:16:56 PM

Title: 3-amino 2-hydroxy benzoic acid =>> preparation
Post by: black_kitty on May 13, 2008, 12:16:56 PM

hi!

I need journal "Monatshefte für Chemie " 1949, vol.80 p.197 and 199
Can any one help me to find this atricle?
or any other journal where I can find preparation of 3-amino 2-hydroxy benzoic acid /another name 3 amino salicylic acid/

Title: Re: 3-amino 2-hydroxy benzoic acid =>> preparation
Post by: sjb on May 13, 2008, 01:01:04 PM

Polyhedron, 2006, 25, 753 uses it, but I don't have full access, so I don't know whether they buy it (pricey) or make it ( http://dx.doi.org/10.1016/j.poly.2005.07.034 )

Perhaps Beilstein, 1931, H14, 579, from http://ecsoc2.hcc.ru/ecsoc-2/a0014/a0014.htm (ref 17) ?

How much do you need? http://www.prosynth.com/exstock.php claim to have 25g of the title compound - but not sure of purity or how recently stock was updated

Just a few random thoughts

S

Title: Re: 3-amino 2-hydroxy benzoic acid =>> preparation
Post by: black_kitty on May 13, 2008, 02:00:15 PM

I must prepare "literature compound" and I shoul include there as many information as I can find.

I have many articles about it prporeties and another compounds in which "my" substance is used but I can't find preparation of my compound.