Chemical Forums
Chemistry Forums for Students => Organic Chemistry Forum => Organic Chemistry Forum for Graduate Students and Professionals => Topic started by: Che_Miss_try on May 16, 2014, 12:43:01 PM
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I am trying to purify and characterize a novel product in methanol. I am a non thesis masters student in a lab with minimal resources. I have been able to characterize the product through NMR after some crystal formation but the product is soluble in everything and I can not remove the impurities. My adviser wants me to figure out how to create a salt precipitate. I have tried to acidify the product out of solution with no luck.
Any suggestions on how I can purify or precipitate my product? Organic is not my strong suit so any topics that I can further research would be a great help. Thank you.