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Chemistry Forums for Students => Organic Chemistry Forum => Topic started by: The Guy on April 15, 2015, 06:57:19 PM

Title: triturated question
Post by: The Guy on April 15, 2015, 06:57:19 PM

I have not tried trituration before, and really do not know how can I do it. I want to follow this procedure:

Quote

After the reaction, water was added and solid formed was filtered. The resulting solid formed was triturated with hexane:ethyl acetate (10–30%), filtered and dried

The Hexane is desolvent for my product, but it is fairly soluble in ethyl acetate. I do not want to lose what I have, and I am afraid my product will get dissolved.