Chemical Forums
Chemistry Forums for Students => Analytical Chemistry Forum => Topic started by: skunny on December 12, 2018, 04:37:30 AM
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Hey
I was really hoping somebody could help me out here, because i have no clue anymore what Else to try...
I am trying to seperate Ethyl-4-hydroxybenzoat and ethylvanillin....i Just don't find the right Solvent mixture....I have a good seperation between those substances, but only If i use ammonia and evaporating ammonia by a rotary evapirator doesnt work Out so Well...does anyone have an idea how i might successful:/? Thx!!!
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I have used rotary evaporation to remove aqueous ammonia on many occasions. If it is not completely removed on the first pass, sometimes redissolving in a solvent and rotovapping again is necessary. Triethylamine is an alternative, I suppose.
Sometimes removal of one solvent is aided by adding a second solvent to strip away the first. I don't have any specific suggestions regarding ammonia in that regard, however.
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Running the column with triethylamine or ammonia then doing an aqueous acid extraction at the end seems reasonable.