Chemical Forums
Chemistry Forums for Students => Analytical Chemistry Forum => Topic started by: Biostartup on February 19, 2019, 07:12:11 PM
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Hi all,
I'm new to the forums and just wanted a second take on my concerns about using sodium azide (powder form).
Occasionally I have to add small amount of sodium azide in powder form to a solution to use as a preservative (0.04-0.08g).
I use an analytical scale (with the slide-able glass "walls").
My PPE is nitrile gloves, lab coat, and a face mask to prevent inhalation through dust generation. I try to isolate any handling of the chemical to within the analytical scales glass.
Is this sufficient for such small amount? After adding some today I just became worried because I've read the SDS and know how dangerous this stuff is. Or am I over-reacting here?
Any advice is welcome, thanks!
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I work with sodium azide in small amounts, and I usually don't use a mask. But your precautions sound good.
The main trick of the trade is to not use a metal spatula. Use a plastic spoon to weigh it.
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What is the problem with the metal spatula?
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What is the problem with the metal spatula?
If memory serves me well it can catalyze explosion of azides.
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Sodium azide isn't very sensitive, but say, chromium or iron azide is. You can create those on the surface of a stainless steel spatula by ion exchange.