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Organic Chemistry Forum for Graduate Students and Professionals / Handling and storing fuming nitric acid
« Last post by Babcock_Hall on Today at 11:06:28 AM »In a month or so, we will be using fuming nitric acid for the first time. We will nitrate a derivative of thiophene on a small scale (50-100 mg?) based on a similar reaction in the literature. If it goes well, we will scale the reaction up to 250-500 mg. We will use oven-dried glassware and a nitrogen atmosphere.
(1) Is there anything special in handling this reagent?
(2) After we open the reagent container, how should we store it? I was thinking of using a small desiccator with some calcium sulfate (Drierite), to minimize its picking up water.
(1) Is there anything special in handling this reagent?
(2) After we open the reagent container, how should we store it? I was thinking of using a small desiccator with some calcium sulfate (Drierite), to minimize its picking up water.