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Alternative solvent to Glycol/Diethyleneglycol for Wolff-Kishner Reduction

Started by zuriel | Last post by zuriel February 22, 2014, 10:27:16 AM

2 Replies
3273 Views
Last post February 22, 2014, 10:27:16 AM
by zuriel
Acylation of 7-azaindole at the C-3 position.

Started by zuriel | Last post by zuriel December 05, 2012, 06:11:22 PM

3 Replies
4362 Views
Last post December 05, 2012, 06:11:22 PM
by zuriel
Cleaving a pivalate ester

Started by zuriel | Last post by SDVENHI April 19, 2014, 02:43:29 AM

5 Replies
4153 Views
Last post April 19, 2014, 02:43:29 AM
by SDVENHI
Any practical tips on using neat boron tribromide?

Started by zuriel | Last post by zuriel April 19, 2016, 05:28:26 AM

5 Replies
4842 Views
Last post April 19, 2016, 05:28:26 AM
by zuriel
Any useful tips for cooling to -10 degC

Started by zuriel | Last post by P January 23, 2018, 08:40:18 AM

5 Replies
5271 Views
Last post January 23, 2018, 08:40:18 AM
by P
Functionalization of 1-naphthylacetic acid

Started by zuriel | Last post by zuriel April 19, 2016, 05:28:08 AM

4 Replies
3555 Views
Last post April 19, 2016, 05:28:08 AM
by zuriel
Procedure for the destruction and disposal of sodium cyanoborohydride

Started by zuriel | Last post by zuriel January 22, 2018, 05:14:57 AM

2 Replies
4422 Views
Last post January 22, 2018, 05:14:57 AM
by zuriel
Recrystallisation Practical Advice

Started by zuriel | Last post by 408 July 03, 2013, 12:35:35 AM

5 Replies
9844 Views
Last post July 03, 2013, 12:35:35 AM
by 408
Removing DMF from a sample of a salt.

Started by zuriel | Last post by Optimist January 30, 2017, 04:40:55 AM

4 Replies
4248 Views
Last post January 30, 2017, 04:40:55 AM
by Optimist
Any tips for removing acetic acid from an oil?

Started by zuriel | Last post by ThePostDoc April 10, 2014, 09:58:00 AM

12 Replies
13245 Views
Last post April 10, 2014, 09:58:00 AM
by ThePostDoc
Boron Trifluoride Dimethylcarbonate

Started by zuriel | Last post by TheUnassuming April 08, 2014, 04:15:47 PM

1 Replies
2512 Views
Last post April 08, 2014, 04:15:47 PM
by TheUnassuming
Synthesis of 3-indolyl skatyl ketone

Started by zuriel | Last post by zuriel June 12, 2014, 05:59:12 AM

10 Replies
6573 Views
Last post June 12, 2014, 05:59:12 AM
by zuriel
Can you make fuming nitric acid from 65% HNO3 and conc. sulphuric?

Started by zuriel | Last post by zuriel January 28, 2015, 07:45:20 PM

6 Replies
4181 Views
Last post January 28, 2015, 07:45:20 PM
by zuriel
Need advice synthesizing 7-Azaindole-3-acetic acid

Started by zuriel | Last post by zuriel January 11, 2014, 09:55:00 PM

10 Replies
6990 Views
Last post January 11, 2014, 09:55:00 PM
by zuriel
Quick question about forming oxoacetic acit derivative of 7-azaindole

Started by zuriel | Last post by zuriel October 23, 2012, 05:57:44 AM

9 Replies
5848 Views
Last post October 23, 2012, 05:57:44 AM
by zuriel
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