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Equipment question: Metered addition to a reaction flask under vacuum

Started by Reddart | Last post by rolnor October 04, 2022, 03:01:41 AM

3 Replies
1762 Views
Last post October 04, 2022, 03:01:41 AM
by rolnor
Solubility of perfluoro alkyl compounds, oxidation etc.

Started by Reddart | Last post by Archer September 03, 2015, 02:32:08 AM

1 Replies
2351 Views
Last post September 03, 2015, 02:32:08 AM
by Archer
Methylating a tertiary amine with MeI in the presence of a carboxylic acid or OH

Started by Reddart | Last post by pgk January 14, 2017, 08:14:59 AM

11 Replies
5385 Views
Last post January 14, 2017, 08:14:59 AM
by pgk
Purity of acid chlorides from thionyl chloride

Started by Reddart | Last post by phth January 26, 2021, 03:27:58 PM

10 Replies
2617 Views
Last post January 26, 2021, 03:27:58 PM
by phth
Protecting N,N-Diisopropylethanolamine, THP?

Started by Reddart | Last post by kriggy July 07, 2016, 05:54:38 PM

2 Replies
2392 Views
Last post July 07, 2016, 05:54:38 PM
by kriggy
Aryl diazonium aryl coupling in THF

Started by Reddart | Last post by opsomath October 02, 2018, 11:04:49 AM

5 Replies
4099 Views
Last post October 02, 2018, 11:04:49 AM
by opsomath
Dialysis purification of ions

Started by Reddart | Last post by Arkcon July 06, 2016, 06:34:22 PM

1 Replies
2459 Views
Last post July 06, 2016, 06:34:22 PM
by Arkcon
Speaking of N-BOC deprotection..

Started by Reddart | Last post by Reddart July 16, 2015, 04:08:39 PM

8 Replies
7713 Views
Last post July 16, 2015, 04:08:39 PM
by Reddart
Any recommendations for auto/semiauto flash sytems?

Started by Reddart | Last post by BobfromNC July 15, 2015, 05:03:41 PM

4 Replies
3997 Views
Last post July 15, 2015, 05:03:41 PM
by BobfromNC
Removing trace metals in aq wash Primarily (Fe)

Started by Reddart | Last post by phth February 19, 2023, 01:27:27 AM

4 Replies
1070 Views
Last post February 19, 2023, 01:27:27 AM
by phth
Suzuki coupling, minimizing byproduct/unreacted iodide

Started by Reddart | Last post by alphahydroxy June 17, 2009, 10:10:18 AM

2 Replies
7878 Views
Last post June 17, 2009, 10:10:18 AM
by alphahydroxy
Friedel-Crafts acylation of BOC-aniline

Started by Reddart | Last post by pgk July 02, 2015, 11:20:33 AM

3 Replies
3305 Views
Last post July 02, 2015, 11:20:33 AM
by pgk
Has anyone bis protected o-phenylene diamine?

Started by Reddart | Last post by pgk July 02, 2015, 11:18:36 AM

14 Replies
6976 Views
Last post July 02, 2015, 11:18:36 AM
by pgk
ethynyltrimethylsilyl stable to Hartwig (NaOtBu)?

Started by Reddart | Last post by Reddart May 21, 2018, 04:00:45 PM

3 Replies
3552 Views
Last post May 21, 2018, 04:00:45 PM
by Reddart
Quaternary ammonium synthesis and counter-ion exchange

Started by Reddart | Last post by Reddart May 05, 2016, 07:05:39 PM

9 Replies
6526 Views
Last post May 05, 2016, 07:05:39 PM
by Reddart
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