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Topic: Catechol tailing on TLC  (Read 1545 times)

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Offline emyonee

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Catechol tailing on TLC
« on: January 03, 2016, 12:42:59 PM »
Hello I'm trying to synthesis a product (which is more polar) from catechol. The problem is catechol (dissolved in methanol) always tails when I spot it on a silica TLC plate. With this I won't be able to tell if there was any product formed in the reaction. I have tried increase the polarity of the mobile phase and reduced the concentration of catechol but still same thing. What can I do to stop the taling?

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