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Topic: Obtaining the final product  (Read 826 times)

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Offline Nathan

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Obtaining the final product
« on: June 08, 2020, 11:13:23 AM »
I obtained this product after a diels alder reaction. The next step is MeONa/MeOh. How could you get the final product from it?
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Offline AWK

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Re: Obtaining the final product
« Reply #1 on: June 08, 2020, 12:22:21 PM »
The reaction of furfuryl alcohol with maleic anhydride varies depending on the conditions and solvent.
Are you sure you have received exo- or endo-III or a mixture of both isomers?
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Offline Nathan

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Re: Obtaining the final product
« Reply #2 on: June 08, 2020, 01:21:20 PM »
I have assumed that the mixture of the two isomers is obtained favoring the product exo- by heat. How should I go from there?
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Offline AWK

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Re: Obtaining the final product
« Reply #3 on: June 08, 2020, 01:49:35 PM »
Heating produces polymers. The reaction is carried out at room temperature for a week. A solvent is also very important. Did you have any specific recipes? Assuming you have the exo-isomer in the last reaction you will receive probably 7-carboxyphtalide.
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