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Topic: gravimetric determinetion of iron(III)  (Read 1394 times)

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Offline filip jovic

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gravimetric determinetion of iron(III)
« on: November 28, 2020, 07:58:22 AM »
hello,
for my thesis i have to determen the iron percentage in a sample using gravimetry. i know this is a homogeneous precipitation, but i dony know the theory behind this, can someone explain this to me and how to do it in the lab.

Offline chenbeier

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Re: gravimetric determinetion of iron(III)
« Reply #1 on: November 28, 2020, 09:18:38 AM »
1. You get weight of your sample.
2. Dissolve it in water, acid, etc.
3. Do a chemical reaction by adding something that the iron precipitate
4.Filter it and dry it
5. Get weight of it, calculate to Fe
6. Quotient of this weight to sample weight times 100 gives percentage
« Last Edit: November 28, 2020, 10:12:05 AM by chenbeier »

Offline filip jovic

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Re: gravimetric determinetion of iron(III)
« Reply #2 on: November 29, 2020, 04:14:51 AM »
thank you for the instructions. but can you explain the theory behind it, i have to give the theory aswell but i dont re&ally understand it that well

Offline AWK

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Re: gravimetric determinetion of iron(III)
« Reply #3 on: November 29, 2020, 05:08:56 AM »
Search textbooks, handbooks, and original literature. Maybe even the internet will help.
AWK

Offline filip jovic

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Theory precipitation iron
« Reply #4 on: November 29, 2020, 06:39:48 AM »
Hello,
I have to determine the iron3+ in a monster. The procedure is: i have to take 0,800 gram of my monster, add 50 ml water and 2 ml HCl then i have to heat it till boiling point then add 1 ml HNO3. And lengthen it to 200 ml. Then i have to add 20 ml NH3 very slowly. Etc..

My question is what is the theory behind this particular precipitation. Can someone explain this to me. It is for my thesis

Offline mjc123

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Re: Theory precipitation iron
« Reply #5 on: November 29, 2020, 07:02:15 AM »
What's your monster? King Kong? Godzilla? We need to know in order to explain the theory.

Seriously though, if you're writing a thesis, a elementary part of the work for your thesis is to learn the theory behind what you're doing. We're not here to do your work for you. Anyway, how much theory is there behind a precipitation? You make something insoluble, it precipitates.

Offline filip jovic

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theory of Gravimetric analysis
« Reply #6 on: November 29, 2020, 07:32:53 AM »
can someone explain fully the theory of Gravimetric analysis.

Offline billnotgatez

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Re: theory of Gravimetric analysis
« Reply #7 on: November 29, 2020, 10:19:17 AM »
This is a question that is complex
Try this WIKI
Gravimetric analysis
https://en.wikipedia.org/wiki/Gravimetric_analysis

Come back with what parts you do not understand and your thoughts


Offline billnotgatez

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Re: gravimetric determinetion of iron(III)
« Reply #8 on: November 29, 2020, 10:28:17 AM »
I have merged all your threads on this topic since they are all similar.

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« Last Edit: November 29, 2020, 10:59:17 AM by billnotgatez »

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