April 17, 2021, 11:07:17 PM
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Topic: storing a hexanes solution of Dibal-H at various temperatures  (Read 156 times)

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Offline Babcock_Hall

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We just used this today using dry syringe technique and nitrogen.  Ever the optimists, we would like to store it for future use.  We plan to put it into a small desiccator.  Is there any advantage in storing at 4° C?  Is -20 °C better?

Offline rolnor

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Re: storing a hexanes solution of Dibal-H at various temperatures
« Reply #1 on: March 30, 2021, 03:41:20 PM »
I think I used it as a DCM-solution, this was an old bottle but worked fine so maybe its not so critical. It was stored in freezer.
Does it say anything on the bottle about storage temp?
What I see itshould be 2-8°C
https://www.sigmaaldrich.com/catalog/product/aldrich/214973?lang=en&region=SE
« Last Edit: March 30, 2021, 04:09:19 PM by rolnor »

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