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6 Amino Penicillianic acid project
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Topic: 6 Amino Penicillianic acid project (Read 1031 times)
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nickgamer49
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6 Amino Penicillianic acid project
«
on:
February 28, 2022, 07:48:30 AM »
Hey! I am new to research and I am trying a project on the condensation to form
phenylpenicillin
(
https://pubchem.ncbi.nlm.nih.gov/compound/6-_Benzoylamino_penicillanic-acid
)
from 6-APA
(
https://pubchem.ncbi.nlm.nih.gov/compound/6-Aminopenicillanic-acid#section=Crystal-Structures
).
I essentially mix 6apa dissolved in basic aqueous solution and benzoyl chloride in propanone to make the product. Because our lab doesnt have any spectroscopes and such, I acidify the solution and separate it with ethyl ethanoate. I am getting really bad yield with this process and a lot is hard to control. Does anyone have a better method or even a different topic involving the chemistry of 6APA? Thanks so much!
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billnotgatez
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Re: 6 Amino Penicillianic acid project
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February 28, 2022, 07:57:46 AM »
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6 Amino Penicillianic acid project