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Topic: Phenol from Anisol with HBr 48%  (Read 967 times)

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Offline Qxir09

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Phenol from Anisol with HBr 48%
« on: September 04, 2023, 01:25:00 PM »
Hello,
i want to make Phenol from Anisol with HBr 48% (i don't have HI, i have AlCl3 but no Chorobenzene).
As far as i know, it doesn't work at room temp.

How long should i reflux and at which temp?

Offline Babcock_Hall

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Re: Phenol from Anisol with HBr 48%
« Reply #1 on: September 05, 2023, 01:28:53 PM »
Do you have access to SciFinder or an equivalent tool?  This would be the best way to obtain conditions.  Why do you want to make something that you can buy?

Offline rolnor

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Re: Phenol from Anisol with HBr 48%
« Reply #2 on: September 15, 2023, 10:23:54 PM »
It usually takes 1hour.

Offline rolnor

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Re: Phenol from Anisol with HBr 48%
« Reply #3 on: September 17, 2023, 04:08:46 AM »
And reflux gives you the right temp.

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