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Topic: Oxidation of 14 with hydrogen peroxide to give the threonic acid derivative 15  (Read 2456 times)

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Offline noda

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Oxidation of 14 with hydrogen peroxide to give the threonic acid derivative 15
« on: November 21, 2006, 03:13:12 PM »
at the beginning was treated with calcium carbonate, afterwards was cooled in an ice bath, and 30% aqueous hydrogen peroxide.
at the end to reaction mixture was added charcoal (DARCO G-60, Fisher) and 10% Pd/C.
1)what is the mechanism of the oxidation (please give in detail) ?
2)why was added charcoal (DARCO G-60, Fisher) and 10% Pd/C a the end of the reaction ?
thank you
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