April 28, 2024, 12:25:15 PM
Forum Rules: Read This Before Posting


Topic: Distillation and exp.(prepare the chloride salt of methy-1-amine  (Read 2993 times)

0 Members and 1 Guest are viewing this topic.

Offline timchai

  • Regular Member
  • ***
  • Posts: 47
  • Mole Snacks: +0/-7
how can we ensure that distillation is finished for b.p. about 120 degre..cel.
do we need to check the b.p. during exp. about the range or other method :'(
and also for another exp , we want to prepare the chloride salt of  methy-1-amine
we place acetamide and bromine,then add NaOH, shake it in cool water , yellow solution is formed
i don't know wt occur during this process :'( and also why do we need to shake in cool water, it decrease the rx rate  :'
in fact i think it produce C3COBr , as i think amide react with OH - ,gv out NH3 ,but i want to ask it should be hjeated, to boil away NH3 , shift eqm ,so i get lost :'(
then the solution is heated and add to NaOH and distillate , to gv product and pass it to HCl , i want to ask wt occur during process ??? and why inveryed funnel is used this time for the product go to HCl ???

Offline Borek

  • Mr. pH
  • Administrator
  • Deity Member
  • *
  • Posts: 27665
  • Mole Snacks: +1801/-410
  • Gender: Male
  • I am known to be occasionally wrong.
    • Chembuddy
Re: Distillation and exp.(prepare the chloride salt of methy-1-amine
« Reply #1 on: March 08, 2009, 05:39:30 AM »
Plain English please.
ChemBuddy chemical calculators - stoichiometry, pH, concentration, buffer preparation, titrations.info

Offline lutesium

  • Full Member
  • ****
  • Posts: 304
  • Mole Snacks: +8/-24
Re: Distillation and exp.(prepare the chloride salt of methy-1-amine
« Reply #2 on: March 14, 2009, 12:34:34 PM »
Please use plain english and tell whatever you want to chronologically event after event not in such a hurry. OK?


Lutesium...

Sponsored Links