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Topic: TREN purification  (Read 4688 times)

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Offline Cheemistree8889

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TREN purification
« on: April 07, 2009, 07:09:58 PM »
I was wondering if anyone has ever distilled TREN?  I found a purification by making the HCl salt but I would much rather distill it.  A method or reference would be great.

Thanks!

Offline Arkcon

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Re: TREN purification
« Reply #1 on: April 07, 2009, 07:39:58 PM »
Can you identify the substance you're interested in without an acronym?  A quick google search for "TREN" identifies it as an anabolic steroid.  We have a policy, on this board, of not giving procedures involving narcotics, medicines, or explosives.
Hey, I'm not judging.  I just like to shoot straight.  I'm a man of science.

Offline Cheemistree8889

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Re: TREN purification
« Reply #2 on: April 07, 2009, 07:45:44 PM »
Tris(2-aminoethyl)amine...it's an encapsulating ligand.


http://en.wikipedia.org/wiki/Tris(2-aminoethyl)amine

Offline ARGOS++

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Re: TREN purification
« Reply #3 on: April 07, 2009, 08:02:55 PM »

Dear Cheemistree8889;

"Your" Wikipedia page tells you that you easily should be able to do an inert vacuum-distillation, what will lower your Bp. from 265°C to approximately 160°C, depending on the vacuum you are able to reach.

Good Luck!
                    ARGOS++

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