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Topic: Analytical method for analysis of mixture of Hydrazines  (Read 3109 times)

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Offline tsragu

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Analytical method for analysis of mixture of Hydrazines
« on: August 27, 2011, 08:00:12 AM »
Dear Members,

I would like to have a reliable method for the analysis of mixture of Hydrazines in aqueous soultion.

The same is mixture of methyl and ethyl hydrazine along with ammonia and unsubstituted hydrazine.

I am comfortable to use HPLC or GC.

tsragu
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Offline marquis

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Re: Analytical method for analysis of mixture of Hydrazines
« Reply #1 on: August 28, 2011, 09:32:33 AM »
I would suggest a nitrogen phosphorus sulfur (NPS) detector for your GC.

I haven't used them for the compounds you are listing.  However, the NPS detector did well for N-nitrosamines. The vendor of the detector should be able to give you more information.

Hope this helps and good luck.
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Offline Stepan

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Re: Analytical method for analysis of mixture of Hydrazines
« Reply #2 on: September 04, 2011, 07:32:17 PM »
You can derivatize them with an aldehyde and test by HPLC-UV
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