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To be perfectly honest if the product is not a solid and more or less thermally stable, Kugelrohr is superior to chromatography as a purification method. One of labmates swears by it and I think he purified 90% of his substrates this way. (I've read a couple of Org Syn preps where they even purify solids (!) by Kugelrohr. Of course you'll need a very good vacuum pump (<0.1 Torr) to pull off something like that)
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