November 14, 2019, 10:41:57 AM
Forum Rules: Read This Before Posting


Topic: Another spectrum problem  (Read 2065 times)

0 Members and 1 Guest are viewing this topic.

Offline adinfinitum

  • New Member
  • **
  • Posts: 6
  • Mole Snacks: +0/-0
Another spectrum problem
« on: January 26, 2014, 08:18:45 PM »
So I'm having problems with an additional set of spectrums.

On the NMR Spectrum the area that I have labelled 3, there seems to be a tiny blip but I think it corresponds to the secondary amine that the IR spectrum proves has to be there. The integration for the blip gives it 1 hydrogen and it fits the area for an amine. Am I off base on assuming this, because it is very tiny relatively?

Link to spectrums: http://imgur.com/a/AyUDb#1

Offline adinfinitum

  • New Member
  • **
  • Posts: 6
  • Mole Snacks: +0/-0
Re: Another spectrum problem
« Reply #1 on: January 26, 2014, 09:35:37 PM »
So I went with my assumption and got N-Isopropylpropan-2-amine as the compound, does this correspond well?

Offline discodermolide

  • Chemist
  • Sr. Member
  • *
  • Posts: 5038
  • Mole Snacks: +404/-70
  • Gender: Male
    • My research history
Re: Another spectrum problem
« Reply #2 on: January 27, 2014, 06:17:08 AM »
That suggestion seems ok, this is the compound you mean?
CC(NC(C)C)C
Development Chemists do it on Scale, Research Chemists just do it!
My Research History

Offline adinfinitum

  • New Member
  • **
  • Posts: 6
  • Mole Snacks: +0/-0
Re: Another spectrum problem
« Reply #3 on: January 27, 2014, 11:00:33 AM »
Yes.

Sponsored Links