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Topic: "Oiling out' synthesis frustrations  (Read 8201 times)

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Offline foxfourfive

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Re: "Oiling out' synthesis frustrations
« Reply #15 on: July 31, 2016, 11:08:52 PM »
So trapped water within the sample was the problem it didn't crystallize? Would you be able to re-crystallize it now?

Yes, once the water was boiled off with Toluene the sample crystallized. It actually started crystallizing in the toluene rapidly once around 20% of the water was boiled off, and it was recrystallized from acetone.

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