You sir are a wizard!
That worked, not the cleanest reaction I have ever done but better than anything else I tried. There is a peak at 3.0-3.05 (it is in CDCl3) which is a broad singlet that integrates to 0.5, I just can not seem to figure out what it is. Granted my NMR sample was very concentrated but I am not sure if I dilute it if that will be cheating if it goes away or integrates to like 0.1. This compound needs to be at least 95% pure. I can try recolumning it but I barely have any left and it is hard to make. Any idea what it might be, I have no alcohols or anything of that sort in the SM, there is no SM left actually and it is one spot by UV. Stained with multiple things and nadaa so I am not sure where it is coming from. The solvent (CDCl3) is also relatively new.