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Topic: Anhydrous HCL gas  (Read 2124 times)

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Offline Biahbi

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Anhydrous HCL gas
« on: November 04, 2014, 08:33:34 PM »
I need to generate anhydrous HCL gas. I know that there are several methods to do this. The most important factor is how dry the gas will be. The second most important factor is keeping the cost down. Dehydraying conc. HCL acid with CaCL2 is the method which appeals to me most. My question is, would the use of a sufficient amount of CaCL2 fully dehyrdate the liquid, releasing the gas, i.e. I won't have to pass the gas through a drying tube or another flask containing conc. sulfuric acid? If the CaCL2 route is not ideal for eliminating all of the water, which method should I use?

Offline Hunter2

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Re: Anhydrous HCL gas
« Reply #1 on: November 05, 2014, 01:14:59 AM »
Better is to create the gas by chemical reaction  PCl3, PCl5 and water or melt NaCl and NaHSO4 together. Dry with phosphorous pent oxide.

Offline discodermolide

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Re: Anhydrous HCL gas
« Reply #2 on: November 05, 2014, 01:47:08 AM »
It's even easier to buy a cylinder.
Development Chemists do it on Scale, Research Chemists just do it!
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