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Topic: How to gradually increase temperature to 220 while refluxing?  (Read 1241 times)

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Offline auxinz

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How to gradually increase temperature to 220 while refluxing?
« on: September 15, 2015, 05:39:15 PM »
I am working on a synthesis reaction of a indole related compound.  The reaction mixture needs to be gradually heated (2 degrees/min) to 220 degrees and then refluxed for 23 hours.  My lab has a GlasCol RampTrol temp controller that uses a thermocouple to measure temperature.  Would situating the thermocouple between the flask and heating mantle work well enough to get the gradual heating required or would I need a different type of measuring device?

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