April 28, 2024, 04:38:37 AM
Forum Rules: Read This Before Posting


« previous next »
Pages: [1]   Go Down

Topic: making HCL-DIOXANE please help  (Read 10636 times)

0 Members and 1 Guest are viewing this topic.

Offline Snake

  • Regular Member
  • ***
  • Posts: 17
  • Mole Snacks: +0/-1
making HCL-DIOXANE please help
« on: May 31, 2006, 12:19:31 PM »
Anyone out there knows how to make 4M HCL-dioxane from 37% HCL and 1,4-dioxane?

Please help.
Logged

Offline Snake

  • Regular Member
  • ***
  • Posts: 17
  • Mole Snacks: +0/-1
Re: making HCL-DIOXANE please help
« Reply #1 on: June 01, 2006, 03:30:51 AM »

No one replied...found a way to generate the hcl-dioxane, by adding acetyl chloride with methanol to genrate hcl and then add dioxane to it... dono whether it works trying it now =)
Logged

Offline AWK

  • Retired Staff
  • Sr. Member
  • *
  • Posts: 7979
  • Mole Snacks: +555/-93
  • Gender: Male
Re: making HCL-DIOXANE please help
« Reply #2 on: June 01, 2006, 05:27:36 AM »
You ought to use dry gaseous HCl, you can obtain it from  solid NaCl + conc. H2SO4
Logged
AWK
Pages: [1]   Go Up
« previous next »
Sponsored Links