April 19, 2024, 06:07:25 AM
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Topic: CBz protection of amines  (Read 8305 times)

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Offline Sach

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Re: CBz protection of amines
« Reply #15 on: October 18, 2017, 04:55:56 PM »
Yes, I did an H-nmr analysis of the oxalate salt. I also determined the melting point (melt traject) and it was almost the same as in the literature.

Offline rolnor

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Re: CBz protection of amines
« Reply #16 on: October 19, 2017, 05:35:24 AM »
Nice that you have got the 3-aminothiophene. My guess is that the Cbz-ptotected amine should be resonable soluble in organic solvent.

Offline Sach

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Re: CBz protection of amines
« Reply #17 on: October 19, 2017, 12:41:42 PM »
all right

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