How do you guys think recrystallization parameters should be reported? Has anyone come across nice published examples: e.g orgsyn?
e.g. "the oil was diluted with this (x mL) and that (y mL), and seeded. The first crop was taken after [time] (mp= 3-4 ºC) washing with hexanes. The second crop was taken after [time] (mp= 1-2 ºC), and the mother liquor was chromatographed (parameters) to obtain the product (z g, %).