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Topic: Phenol from Anisol with HBr 48%  (Read 1000 times)

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Offline Qxir09

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Phenol from Anisol with HBr 48%
« on: September 04, 2023, 01:25:00 PM »
Hello,
i want to make Phenol from Anisol with HBr 48% (i don't have HI, i have AlCl3 but no Chorobenzene).
As far as i know, it doesn't work at room temp.

How long should i reflux and at which temp?
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Offline Babcock_Hall

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Re: Phenol from Anisol with HBr 48%
« Reply #1 on: September 05, 2023, 01:28:53 PM »
Do you have access to SciFinder or an equivalent tool?  This would be the best way to obtain conditions.  Why do you want to make something that you can buy?
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Offline rolnor

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Re: Phenol from Anisol with HBr 48%
« Reply #2 on: September 15, 2023, 10:23:54 PM »
It usually takes 1hour.
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Offline rolnor

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Re: Phenol from Anisol with HBr 48%
« Reply #3 on: September 17, 2023, 04:08:46 AM »
And reflux gives you the right temp.
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