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Topic: Eliminating Pulse in a Conductivity Detector  (Read 4295 times)

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Offline Bitty

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Eliminating Pulse in a Conductivity Detector
« on: February 27, 2008, 02:16:19 PM »
Has anyone run into problems with a small baseline pulse in a conductivity detector? I'm running a Dionex 2000i Cation Chromatograph and am seeing a baseline pulse of about 0.8 MicroSeimens.

I've tried cleaning the detector with 1N HCl and water, setting the temperature compensation to 0, and even switching in a new detector. Nothing seems to work.  I also know it isn't a power supply problem because I am running anions in series and that detector remains stable.

Any suggestions would be appreciated! Thanks!

Offline Bitty

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Re: Eliminating Pulse in a Conductivity Detector
« Reply #1 on: April 23, 2008, 06:14:48 PM »
If any of the 96 chemists that read this post are interested, we have solved this problem. It was a combination of faulty check valves and pressure transducer. :-)

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